Thermal decomposed behavior and kinetic study for untreated and flame retardant treated regenerated cellulose fibers using thermogravimetric analysis

Journal of Thermal Analysis and Calorimetry - In the present work, pyrolysis kinetic mechanism was studied for regenerated cellulosic fiber (RCF) and composite RCF containing silicon/nitrogen flame...     

Gröbner–Shirshov bases for some Lie algebras

Siberian Mathematical Journal - We give Gröbner–Shirshov bases for the Drinfeld–Kohno Lie algebra L n in [1] and the Kukin Lie algebra A P in [2], where P is a semigroup. By way of...     

有机物同分异构体的学习进阶研究

分析了高中生学习同分异构体的思维过程,建构碳架异构、位置异构、官能团类型异构、信息加工推理的四维度五水平模型。合理设计学习进阶,系统发展高中同分异构体思维水平,得到三学段五层级十二进阶设计。系统规划进阶,精准评价思维,建议使用结构模型和思维导图进行教学,发展学生同分异构体的思维水平,培养学生模型认知的核心素养。     

The preparation of ionic liquid based iron phosphate/CNTs composite via microwave radiation for hydrogen evolution reaction and oxygen evolution reaction

Water electrolysis is a promising method for hydrogen production, so the preparation of low-cost and efficient electrocatalysts with a quick and simple procedure is crucial. Herein, iron phosphate (Fe₇(PO₄)₆) was prepared via microwave radiation using ionic liquid (IL) as iron and phosphorus dual-source. This method is simple and rapid, and the product can be directly used as electrocatalysts without further treatment. The experimental results show that the IL can influence the morphology and electrocatalytic performance. Moreover, the addition of carbon nanotubes (CNTs) is favorable for formation of iron phosphate nanoparticles to improve the catalytic activities. As hydrogen evolution reaction (HER) catalyst, this iron phosphate/CNTs exhibits an onset overpotential of 120 mV, Tafel slope of 32.9 mV dec^-1, and current densities of 10 mA cm⁻² at overpotential of 185 mV. Then, it obtains a good activity for oxygen evolution reaction (OER) with a low onset potential of 1.48 V, Tafel slope of 73.3 mV dec^-1, and it only needs an overpotential of 300 mV to drive the 10 mA cm⁻². This bifunctional catalyst also shows good durability for HER and OER. This microwave-assisted method provides an outstanding strategy to prepare iron phosphate in a simple and fast process with good catalytic performance for water splitting.     

乘积拓扑动力系统的转移不变集

研究一般拓扑动力系统的复杂性是很困难的,拓扑共轭、拓扑半共轭、嵌入映射和转移不变集都可以不同程度保持动力系统的复杂性.通过研究拓扑动力系统与符号动力系统拓扑共轭,找到了拓扑动力(子)系统存在转移不变集的条件,同时证明了拓扑动力系统存在转移不变集与乘积拓扑动力系统存在转移不变集的关系,通过研究相对简单、直观的符号动力系统,间接的反应一般拓扑动力(子)系统与其乘积拓扑动力系统的动力性状.     

超声波提取-火焰原子吸收光谱法测定金银花中的Fe、Cu和Pb

建立了湿法和超声波提取处理样品,火焰原子吸收光谱法测定金银花湿法消解液及超声波提取液中Fe,Cu和Pb元素含量的方法.金银花中3种元素的含量Fe＞Cu＞Pb,硝酸作为提取剂,提取元素的溶出率的大小:Cu＞Pb＞Fe,回收率为85％-107％,RSD为0.6-1.0％.结果表明,超声波提取能较好地提取金银花中微量元素,元...     

全序幂等元剩余格

研究了全序幂等元剩余格,给出了全序幂等元剩余格的另一种新的构造方法,并且得到了这类剩余格的结构定理,推广了相关文献的结论．